Ležaja-Zebić, Maja

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  • Ležaja-Zebić, Maja (5)
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Author's Bibliography

Dissimilar sintered calcium phosphate dental inserts as dentine substitutes: Shear bond strength to restorative materials

Ayoub, Giuma; Ležaja-Zebić, Maja; Miletić, Vesna; Petrović, Rada; Veljović, Đorđe; Janaćković, Đorđe

(Wiley, Hoboken, 2020)

TY  - JOUR
AU  - Ayoub, Giuma
AU  - Ležaja-Zebić, Maja
AU  - Miletić, Vesna
AU  - Petrović, Rada
AU  - Veljović, Đorđe
AU  - Janaćković, Đorđe
PY  - 2020
UR  - https://smile.stomf.bg.ac.rs/handle/123456789/1046
AB  - The application of sintered calcium phosphate dental inserts in the central part of tooth cavities can reduce amount of embedded dental composite and polymerization shrinkage of final dental fillings. The aim of this study was to analyze comparatively physico-chemical and mechanical properties of dental inserts and shear bond strength (SBS) between three dissimilar hydroxyapatite-based dental inserts and different restorative materials, after application of different clinical protocols. Starting from two different hydroxyapatite nano powders and nanostructured stabilized zirconia (YSZ), monophasic two-step sintered dense HAp inserts (TSSHAp), biphasic single-step sintered controlled porous inserts (HAp/TCp), and single-step sintered reinforced HAp/YSZ inserts were processed and characterized. Obvious differences in the microstructure of inserts surface were visualized after etching with 37% phosphoric acid. Fracture toughness of sintered inserts was ranged between 1.01 and 1.85 MPam(1/2) (maximum value in the case of HAp/YSZ), while hardness values were in the range of 3.71-5.22 GPa (maximum value in the case of TSSHAp). Acid etching before application improved SBS between inserts and Maxcem compared to direct cement application. TSSHAp and HAP/TCp inserts showed comparable and relatively high SBS values, certainly higher compared to HAp/YSZ inserts. Slightly higher SBS values were measured in the case of TSSHAp insert group, and the highest mean SBS value of 18.51 MPa was determined between TSSHAp inserts and Filtek Z250_SBU following the "self-etch" protocol.
PB  - Wiley, Hoboken
T2  - Journal of Biomedical Materials Research Part B: Applied Biomaterials
T1  - Dissimilar sintered calcium phosphate dental inserts as dentine substitutes: Shear bond strength to restorative materials
DO  - 10.1002/jbm.b.34578
ER  - 
@article{
author = "Ayoub, Giuma and Ležaja-Zebić, Maja and Miletić, Vesna and Petrović, Rada and Veljović, Đorđe and Janaćković, Đorđe",
year = "2020",
abstract = "The application of sintered calcium phosphate dental inserts in the central part of tooth cavities can reduce amount of embedded dental composite and polymerization shrinkage of final dental fillings. The aim of this study was to analyze comparatively physico-chemical and mechanical properties of dental inserts and shear bond strength (SBS) between three dissimilar hydroxyapatite-based dental inserts and different restorative materials, after application of different clinical protocols. Starting from two different hydroxyapatite nano powders and nanostructured stabilized zirconia (YSZ), monophasic two-step sintered dense HAp inserts (TSSHAp), biphasic single-step sintered controlled porous inserts (HAp/TCp), and single-step sintered reinforced HAp/YSZ inserts were processed and characterized. Obvious differences in the microstructure of inserts surface were visualized after etching with 37% phosphoric acid. Fracture toughness of sintered inserts was ranged between 1.01 and 1.85 MPam(1/2) (maximum value in the case of HAp/YSZ), while hardness values were in the range of 3.71-5.22 GPa (maximum value in the case of TSSHAp). Acid etching before application improved SBS between inserts and Maxcem compared to direct cement application. TSSHAp and HAP/TCp inserts showed comparable and relatively high SBS values, certainly higher compared to HAp/YSZ inserts. Slightly higher SBS values were measured in the case of TSSHAp insert group, and the highest mean SBS value of 18.51 MPa was determined between TSSHAp inserts and Filtek Z250_SBU following the "self-etch" protocol.",
publisher = "Wiley, Hoboken",
journal = "Journal of Biomedical Materials Research Part B: Applied Biomaterials",
title = "Dissimilar sintered calcium phosphate dental inserts as dentine substitutes: Shear bond strength to restorative materials",
doi = "10.1002/jbm.b.34578"
}
Ayoub, G., Ležaja-Zebić, M., Miletić, V., Petrović, R., Veljović, Đ.,& Janaćković, Đ.. (2020). Dissimilar sintered calcium phosphate dental inserts as dentine substitutes: Shear bond strength to restorative materials. in Journal of Biomedical Materials Research Part B: Applied Biomaterials
Wiley, Hoboken..
https://doi.org/10.1002/jbm.b.34578
Ayoub G, Ležaja-Zebić M, Miletić V, Petrović R, Veljović Đ, Janaćković Đ. Dissimilar sintered calcium phosphate dental inserts as dentine substitutes: Shear bond strength to restorative materials. in Journal of Biomedical Materials Research Part B: Applied Biomaterials. 2020;.
doi:10.1002/jbm.b.34578 .
Ayoub, Giuma, Ležaja-Zebić, Maja, Miletić, Vesna, Petrović, Rada, Veljović, Đorđe, Janaćković, Đorđe, "Dissimilar sintered calcium phosphate dental inserts as dentine substitutes: Shear bond strength to restorative materials" in Journal of Biomedical Materials Research Part B: Applied Biomaterials (2020),
https://doi.org/10.1002/jbm.b.34578 . .
3
3

Fluoride release from conventional, resin-modified and hybrid glass ionomer cements

Ležaja-Zebić, Maja; Jakovljević, Nikola; Miletić, Vesna

(Srpsko lekarsko društvo - Stomatološka sekcija, Beograd, 2018)

TY  - JOUR
AU  - Ležaja-Zebić, Maja
AU  - Jakovljević, Nikola
AU  - Miletić, Vesna
PY  - 2018
UR  - https://smile.stomf.bg.ac.rs/handle/123456789/2361
AB  - Introduction the aim of the study was to quantify and compare fluoride release from four different glass ionomer cement products (GICs). Materials and Methods Standardized disk-shaped samples (5x2mm; n=5/group) of GIC restorative materials: conventional (Fuji IX, GC Corp., Japan), resin-modified (Fuji II LC, GC) and hybrid glass ionomer cement (Equia Forte, GC) and a conventional GIC liner/base material (Alfagal, Galenika, Serbia) were tested for fluoride release up to 21 days post-setting. Each sample was immersed in 5 mL of fresh deionized water during each time interval. Universal microhybrid composite (Filtek Z250, 3M EPSE, USA) and adhesive (Adper Single Bond, 3M ESPE) were used as negative controls. Fluoride release was measured using an F-selective electrode (Cole-Parmer, USA) and an ion meter (Oakton 700, Cole-Parmer, USA). Data were statistically analyzed using one-way ANOVA, regression and correlation analysis at 0.05. Results the highest total fluoride release was measured from Alfagal (386±61 ppm/g), and significantly less from Equia (188±29 ppm/g), Fuji IX (143±11 ppm/g) and Fuji II LC (104±14 ppm/g) (p  lt  0.05). All GICs showed the highest fluoride release during the first 24 hours post-setting. After 3 days, fluoride release slowed down reaching a plateau for all materials. Regression and Pearson correlation analysis showed significant inverse relationship between fluoride release and sample mass and density (p lt 0.001). Conclusion of the three GICs indicated for use as restorative materials, Equia Forte released the highest fluoride concentration. Fluoride release was material and density dependent, with higher release occurring from lower density GICs.
AB  - Uvod Cilj ovog istraživanja je bio da se kvantifikuje i uporedi otpuštanje fluorida iz četiri glasjonomer cementa (GJC). Materijal i metode Napravljeni su standardizovani diskovi (5 × 2 mm; n = 5/grupa) od sledećih GJC: konvencionalnih (Fuji IX, GC Corp., Japan), smolom modifikovani (Fuji II LC, GC), hibridni GJC (Equia Forte, GC) i konvencionalni GJC lajner/baza (Alfagal, Galenika, Srbija). Ispitivano je otpuštanje fluorida tokom 21 dana tako što je svaki uzorak potapan u 5 ml sveže destilovane vode posle svakog mernog intervala. Univerzalni mikrohibridni kompozit (Filtek Z250, 3M EPSE, USA) i adheziv (Adper Single Bond, 3M ESPE) korišćeni su kao negativne kontrole. Otpuštanje fluorida je očitavano pomoću fluor-selektivne elektrode (Cole-Parmer, USA) i jon-metra (Oakton 700, Cole-Parmer, USA). Rezultati su statistički obrađeni ANOVA testom, regresionim i korelacionim analizama sa α = 0,05. Rezultati Ukupno otpuštanje fluorida je bilo najveće iz Alfagala (386 ± 61 ppm/g), značajno manje iz Equia Forte (188 ± 29 ppm/g), Fuji IX (143 ± 11 ppm/g), a najmanje iz Fuji II LC (104 ± 14 ppm/g) (p  lt  0,05). Svi GJC pokazali su najveće otpuštanje fluorida u toku prva 24 h po vezivanju. Posle tri dana otpuštanje fluorida je postajalo sporije dostižući plato za sva četiri materijala. Regresiona i Pirsonova korelaciona analiza pokazale su značajan obrnut odnos između otpuštanja fluorida i mase i gustine uzoraka (p  lt  0,001). Zaključak Od GJC indikovanih za ispune, Equia Forte je otpustila najveću koncentraciju fluorida. Otpuštanje fluorida zavisi od materijala i njegove gustine, pri čemu GJC manje gustine otpuštaju više fluorida.
PB  - Srpsko lekarsko društvo - Stomatološka sekcija, Beograd
T2  - Stomatološki glasnik Srbije
T1  - Fluoride release from conventional, resin-modified and hybrid glass ionomer cements
T1  - Otpuštanje fluorida iz konvencionalnih, smolom modifikovanih i hibridnih glas-jonomer cemenata
VL  - 65
IS  - 4
SP  - 187
EP  - 194
UR  - https://hdl.handle.net/21.15107/rcub_smile_2361
ER  - 
@article{
author = "Ležaja-Zebić, Maja and Jakovljević, Nikola and Miletić, Vesna",
year = "2018",
abstract = "Introduction the aim of the study was to quantify and compare fluoride release from four different glass ionomer cement products (GICs). Materials and Methods Standardized disk-shaped samples (5x2mm; n=5/group) of GIC restorative materials: conventional (Fuji IX, GC Corp., Japan), resin-modified (Fuji II LC, GC) and hybrid glass ionomer cement (Equia Forte, GC) and a conventional GIC liner/base material (Alfagal, Galenika, Serbia) were tested for fluoride release up to 21 days post-setting. Each sample was immersed in 5 mL of fresh deionized water during each time interval. Universal microhybrid composite (Filtek Z250, 3M EPSE, USA) and adhesive (Adper Single Bond, 3M ESPE) were used as negative controls. Fluoride release was measured using an F-selective electrode (Cole-Parmer, USA) and an ion meter (Oakton 700, Cole-Parmer, USA). Data were statistically analyzed using one-way ANOVA, regression and correlation analysis at 0.05. Results the highest total fluoride release was measured from Alfagal (386±61 ppm/g), and significantly less from Equia (188±29 ppm/g), Fuji IX (143±11 ppm/g) and Fuji II LC (104±14 ppm/g) (p  lt  0.05). All GICs showed the highest fluoride release during the first 24 hours post-setting. After 3 days, fluoride release slowed down reaching a plateau for all materials. Regression and Pearson correlation analysis showed significant inverse relationship between fluoride release and sample mass and density (p lt 0.001). Conclusion of the three GICs indicated for use as restorative materials, Equia Forte released the highest fluoride concentration. Fluoride release was material and density dependent, with higher release occurring from lower density GICs., Uvod Cilj ovog istraživanja je bio da se kvantifikuje i uporedi otpuštanje fluorida iz četiri glasjonomer cementa (GJC). Materijal i metode Napravljeni su standardizovani diskovi (5 × 2 mm; n = 5/grupa) od sledećih GJC: konvencionalnih (Fuji IX, GC Corp., Japan), smolom modifikovani (Fuji II LC, GC), hibridni GJC (Equia Forte, GC) i konvencionalni GJC lajner/baza (Alfagal, Galenika, Srbija). Ispitivano je otpuštanje fluorida tokom 21 dana tako što je svaki uzorak potapan u 5 ml sveže destilovane vode posle svakog mernog intervala. Univerzalni mikrohibridni kompozit (Filtek Z250, 3M EPSE, USA) i adheziv (Adper Single Bond, 3M ESPE) korišćeni su kao negativne kontrole. Otpuštanje fluorida je očitavano pomoću fluor-selektivne elektrode (Cole-Parmer, USA) i jon-metra (Oakton 700, Cole-Parmer, USA). Rezultati su statistički obrađeni ANOVA testom, regresionim i korelacionim analizama sa α = 0,05. Rezultati Ukupno otpuštanje fluorida je bilo najveće iz Alfagala (386 ± 61 ppm/g), značajno manje iz Equia Forte (188 ± 29 ppm/g), Fuji IX (143 ± 11 ppm/g), a najmanje iz Fuji II LC (104 ± 14 ppm/g) (p  lt  0,05). Svi GJC pokazali su najveće otpuštanje fluorida u toku prva 24 h po vezivanju. Posle tri dana otpuštanje fluorida je postajalo sporije dostižući plato za sva četiri materijala. Regresiona i Pirsonova korelaciona analiza pokazale su značajan obrnut odnos između otpuštanja fluorida i mase i gustine uzoraka (p  lt  0,001). Zaključak Od GJC indikovanih za ispune, Equia Forte je otpustila najveću koncentraciju fluorida. Otpuštanje fluorida zavisi od materijala i njegove gustine, pri čemu GJC manje gustine otpuštaju više fluorida.",
publisher = "Srpsko lekarsko društvo - Stomatološka sekcija, Beograd",
journal = "Stomatološki glasnik Srbije",
title = "Fluoride release from conventional, resin-modified and hybrid glass ionomer cements, Otpuštanje fluorida iz konvencionalnih, smolom modifikovanih i hibridnih glas-jonomer cemenata",
volume = "65",
number = "4",
pages = "187-194",
url = "https://hdl.handle.net/21.15107/rcub_smile_2361"
}
Ležaja-Zebić, M., Jakovljević, N.,& Miletić, V.. (2018). Fluoride release from conventional, resin-modified and hybrid glass ionomer cements. in Stomatološki glasnik Srbije
Srpsko lekarsko društvo - Stomatološka sekcija, Beograd., 65(4), 187-194.
https://hdl.handle.net/21.15107/rcub_smile_2361
Ležaja-Zebić M, Jakovljević N, Miletić V. Fluoride release from conventional, resin-modified and hybrid glass ionomer cements. in Stomatološki glasnik Srbije. 2018;65(4):187-194.
https://hdl.handle.net/21.15107/rcub_smile_2361 .
Ležaja-Zebić, Maja, Jakovljević, Nikola, Miletić, Vesna, "Fluoride release from conventional, resin-modified and hybrid glass ionomer cements" in Stomatološki glasnik Srbije, 65, no. 4 (2018):187-194,
https://hdl.handle.net/21.15107/rcub_smile_2361 .

Composite nanostructured hydroxyapatite/yttrium stabilized zirconia dental inserts - The processing and application as dentin substitutes

Ayoub, Giuma; Veljović, Đorđe; Ležaja-Zebić, Maja; Miletić, Vesna; Palcevskis, Eriks; Petrović, Rada; Janaćković, Đorđe

(Elsevier Sci Ltd, Oxford, 2018)

TY  - JOUR
AU  - Ayoub, Giuma
AU  - Veljović, Đorđe
AU  - Ležaja-Zebić, Maja
AU  - Miletić, Vesna
AU  - Palcevskis, Eriks
AU  - Petrović, Rada
AU  - Janaćković, Đorđe
PY  - 2018
UR  - https://smile.stomf.bg.ac.rs/handle/123456789/2305
AB  - The objective of the study was to process nano-structured hydroxyapatite/yttrium-stabilized zirconia bioceramic and to investigate the possibilities of its application as dentin replacement in the form of dental inserts. The processing conditions were varied in order to optimize phase composition, microstructure, fracture toughness, hardness and shear bond strength (SBS) between the obtained composite inserts and restorative materials, following either the "total-etch" or "self-etch" clinical protocol. Composite nano-powder, obtained by mixing and homogenization of 80 wt% of stoichiometric hydroxyapatite (HAp) synthesized by modified precipitation method and 20wt% of yttrium-stabilized ZrO2 (YSZ) synthesized by plasma method, was isostatically pressed into cylinder-shaped green bodies. After dilatometric analysis, HAp/YSZ inserts were sintered in the temperature range from 1200 degrees C to 1300 degrees C. Hardness and fracture toughness of sintered inserts were ranged between 3.90 +/- 0.20 - 3.95 +/- 0.12 GPa and 1.82 +/- 0.04 - 1.88 +/- 0.03 MPam(1/2), respectively. Microstructural analysis of biphasic HAp/t-ZrO2 inserts indicated two potential fracture mechanisms for fracture toughness increasing. Sintering temperature and different clinical protocols affected SBS between processed inserts and commercial dental restorative materials. Maximum SBS values of 10.50 +/- 4.94 MPa (mean standard deviation) were reached in inserts sintered at 1300 degrees C, following the "self-etch" protocol of adhesive application. It could be concluded that resin-based composites could be strongly bonded to HAp/YSZ inserts, preferably with self-etch" adhesive application. In addition, the values of fracture toughness and hardness of the obtained inserts indicated the possibility of their usage as dentin substitutes, which could be a good prerequisite for satisfactory mechanics of restored teeth.
PB  - Elsevier Sci Ltd, Oxford
T2  - Ceramics International
T1  - Composite nanostructured hydroxyapatite/yttrium stabilized zirconia dental inserts - The processing and application as dentin substitutes
VL  - 44
IS  - 15
SP  - 18200
EP  - 18208
DO  - 10.1016/j.ceramint.2018.07.028
ER  - 
@article{
author = "Ayoub, Giuma and Veljović, Đorđe and Ležaja-Zebić, Maja and Miletić, Vesna and Palcevskis, Eriks and Petrović, Rada and Janaćković, Đorđe",
year = "2018",
abstract = "The objective of the study was to process nano-structured hydroxyapatite/yttrium-stabilized zirconia bioceramic and to investigate the possibilities of its application as dentin replacement in the form of dental inserts. The processing conditions were varied in order to optimize phase composition, microstructure, fracture toughness, hardness and shear bond strength (SBS) between the obtained composite inserts and restorative materials, following either the "total-etch" or "self-etch" clinical protocol. Composite nano-powder, obtained by mixing and homogenization of 80 wt% of stoichiometric hydroxyapatite (HAp) synthesized by modified precipitation method and 20wt% of yttrium-stabilized ZrO2 (YSZ) synthesized by plasma method, was isostatically pressed into cylinder-shaped green bodies. After dilatometric analysis, HAp/YSZ inserts were sintered in the temperature range from 1200 degrees C to 1300 degrees C. Hardness and fracture toughness of sintered inserts were ranged between 3.90 +/- 0.20 - 3.95 +/- 0.12 GPa and 1.82 +/- 0.04 - 1.88 +/- 0.03 MPam(1/2), respectively. Microstructural analysis of biphasic HAp/t-ZrO2 inserts indicated two potential fracture mechanisms for fracture toughness increasing. Sintering temperature and different clinical protocols affected SBS between processed inserts and commercial dental restorative materials. Maximum SBS values of 10.50 +/- 4.94 MPa (mean standard deviation) were reached in inserts sintered at 1300 degrees C, following the "self-etch" protocol of adhesive application. It could be concluded that resin-based composites could be strongly bonded to HAp/YSZ inserts, preferably with self-etch" adhesive application. In addition, the values of fracture toughness and hardness of the obtained inserts indicated the possibility of their usage as dentin substitutes, which could be a good prerequisite for satisfactory mechanics of restored teeth.",
publisher = "Elsevier Sci Ltd, Oxford",
journal = "Ceramics International",
title = "Composite nanostructured hydroxyapatite/yttrium stabilized zirconia dental inserts - The processing and application as dentin substitutes",
volume = "44",
number = "15",
pages = "18200-18208",
doi = "10.1016/j.ceramint.2018.07.028"
}
Ayoub, G., Veljović, Đ., Ležaja-Zebić, M., Miletić, V., Palcevskis, E., Petrović, R.,& Janaćković, Đ.. (2018). Composite nanostructured hydroxyapatite/yttrium stabilized zirconia dental inserts - The processing and application as dentin substitutes. in Ceramics International
Elsevier Sci Ltd, Oxford., 44(15), 18200-18208.
https://doi.org/10.1016/j.ceramint.2018.07.028
Ayoub G, Veljović Đ, Ležaja-Zebić M, Miletić V, Palcevskis E, Petrović R, Janaćković Đ. Composite nanostructured hydroxyapatite/yttrium stabilized zirconia dental inserts - The processing and application as dentin substitutes. in Ceramics International. 2018;44(15):18200-18208.
doi:10.1016/j.ceramint.2018.07.028 .
Ayoub, Giuma, Veljović, Đorđe, Ležaja-Zebić, Maja, Miletić, Vesna, Palcevskis, Eriks, Petrović, Rada, Janaćković, Đorđe, "Composite nanostructured hydroxyapatite/yttrium stabilized zirconia dental inserts - The processing and application as dentin substitutes" in Ceramics International, 44, no. 15 (2018):18200-18208,
https://doi.org/10.1016/j.ceramint.2018.07.028 . .
26
13
23

Microtensile bond strength of universal adhesives to flat versus Class I cavity dentin with pulpal pressure simulation

Ležaja-Zebić, Maja; Dželetović, Bojan; Miletić, Vesna

(Wiley, Hoboken, 2018)

TY  - JOUR
AU  - Ležaja-Zebić, Maja
AU  - Dželetović, Bojan
AU  - Miletić, Vesna
PY  - 2018
UR  - https://smile.stomf.bg.ac.rs/handle/123456789/2299
AB  - Objectives: The aim of this study was to test long-term microtensile bond strength (mu TBS) of 2 universal adhesives applied to dentin following "total-etch" (TE) or "self-etch" (SE) protocols and aged by direct or indirect water exposure using simulated pulpal pressure. Materials and methods: Single Bond Universal (SBU, 3M ESPE) or Ipera Bond (IP, Itena) were applied to mid-coronal dentin ("flat dentin") or Class I cavity ("cavity dentin") following TE or SE protocols in 112 extracted human third molars. Sixteen groups (n=7 per group) were prepared, 8 groups for mu TBS measurements after 24 hours, and further 8 groups for measurements after 6 months storage. "Cavity dentin" groups were subjected to simulated hydrostatic pulpal pressure of 15 cm H2O using a custom-made device before cutting 1 x 1 mm sticks while "flat dentin" groups were cut into sticks and directly exposed to deionized water. Results: Generally, the TE protocol resulted in highest mu TBS values on flat dentin initially for both adhesives (general linear model, P lt .05). Long-term storage resulted in significantly lower mu TBS values for the TE protocol (P lt .05) while the SE protocol showed comparable values after 6 months (P>.05). "Cavity dentin" with simulated pulpal pressure resulted in lower mu TBS than "flat dentin" (P lt .05). For both adhesives, mu TBS was in the range of 19-42 MPa initially and 16-36 MPa after 6 months storage. Conclusions: mu TBS to dentin of universal adhesives is more stable in the long term following the SE than TE protocol. Simulated pulpal pressure and cavity-type sample preparation may be recommended for mu TBS testing as a more clinically relevant strategy.
PB  - Wiley, Hoboken
T2  - Journal of Esthetic & Restorative Dentistry
T1  - Microtensile bond strength of universal adhesives to flat versus Class I cavity dentin with pulpal pressure simulation
VL  - 30
IS  - 3
SP  - 240
EP  - 248
DO  - 10.1111/jerd.12363
ER  - 
@article{
author = "Ležaja-Zebić, Maja and Dželetović, Bojan and Miletić, Vesna",
year = "2018",
abstract = "Objectives: The aim of this study was to test long-term microtensile bond strength (mu TBS) of 2 universal adhesives applied to dentin following "total-etch" (TE) or "self-etch" (SE) protocols and aged by direct or indirect water exposure using simulated pulpal pressure. Materials and methods: Single Bond Universal (SBU, 3M ESPE) or Ipera Bond (IP, Itena) were applied to mid-coronal dentin ("flat dentin") or Class I cavity ("cavity dentin") following TE or SE protocols in 112 extracted human third molars. Sixteen groups (n=7 per group) were prepared, 8 groups for mu TBS measurements after 24 hours, and further 8 groups for measurements after 6 months storage. "Cavity dentin" groups were subjected to simulated hydrostatic pulpal pressure of 15 cm H2O using a custom-made device before cutting 1 x 1 mm sticks while "flat dentin" groups were cut into sticks and directly exposed to deionized water. Results: Generally, the TE protocol resulted in highest mu TBS values on flat dentin initially for both adhesives (general linear model, P lt .05). Long-term storage resulted in significantly lower mu TBS values for the TE protocol (P lt .05) while the SE protocol showed comparable values after 6 months (P>.05). "Cavity dentin" with simulated pulpal pressure resulted in lower mu TBS than "flat dentin" (P lt .05). For both adhesives, mu TBS was in the range of 19-42 MPa initially and 16-36 MPa after 6 months storage. Conclusions: mu TBS to dentin of universal adhesives is more stable in the long term following the SE than TE protocol. Simulated pulpal pressure and cavity-type sample preparation may be recommended for mu TBS testing as a more clinically relevant strategy.",
publisher = "Wiley, Hoboken",
journal = "Journal of Esthetic & Restorative Dentistry",
title = "Microtensile bond strength of universal adhesives to flat versus Class I cavity dentin with pulpal pressure simulation",
volume = "30",
number = "3",
pages = "240-248",
doi = "10.1111/jerd.12363"
}
Ležaja-Zebić, M., Dželetović, B.,& Miletić, V.. (2018). Microtensile bond strength of universal adhesives to flat versus Class I cavity dentin with pulpal pressure simulation. in Journal of Esthetic & Restorative Dentistry
Wiley, Hoboken., 30(3), 240-248.
https://doi.org/10.1111/jerd.12363
Ležaja-Zebić M, Dželetović B, Miletić V. Microtensile bond strength of universal adhesives to flat versus Class I cavity dentin with pulpal pressure simulation. in Journal of Esthetic & Restorative Dentistry. 2018;30(3):240-248.
doi:10.1111/jerd.12363 .
Ležaja-Zebić, Maja, Dželetović, Bojan, Miletić, Vesna, "Microtensile bond strength of universal adhesives to flat versus Class I cavity dentin with pulpal pressure simulation" in Journal of Esthetic & Restorative Dentistry, 30, no. 3 (2018):240-248,
https://doi.org/10.1111/jerd.12363 . .
9
4
10

The effect of calcinated hydroxyapatite and magnesium doped hydroxyapatite as fillers on the mechanical properties of a model bisgma/tegdma dental composite initially and after aging

Matić, Tamara; Ležaja-Zebić, Maja; Cvijović-Alagić, Ivana; Miletić, Vesna; Petrović, Rada; Janaćković, Đorđe; Veljović, Đorđe

(Savez inženjera metalurgije Srbije, Beograd, 2018)

TY  - JOUR
AU  - Matić, Tamara
AU  - Ležaja-Zebić, Maja
AU  - Cvijović-Alagić, Ivana
AU  - Miletić, Vesna
AU  - Petrović, Rada
AU  - Janaćković, Đorđe
AU  - Veljović, Đorđe
PY  - 2018
UR  - https://smile.stomf.bg.ac.rs/handle/123456789/2281
AB  - This study aimed to investigate the possibility of modifying model BisGMA/TEGDMA dental composite by substituting 10 wt. % of conventional glass fillers with bioactive fillers based on calcinated nanosized hydroxyapatite (HAp) and Mg-doped hydroxyapatite (Mg-HAp). HAp and Mg-HAp powders were synthesized hydrothermally. Mechanical properties: hardness by Vickers (HV) and flexural strength (Fs) were tested initially and after being stored for 28 days in simulated body fluid (SBF). The experimental composites with HAp and Mg-HAp particles showed no statistically significant difference in HV compared to the control (p>0.05) either initially or after storage. Although mean Fs values of modified composites tested initially were lower (62 MPa) than those of the control (72 MPa), after 28 days of storage in SBF Fs values were greater for modified composites (42 MPa control sample, 48 MPa HAp, and Mg-HAp samples). In vitro bioactivity of BisGMA/TEGDMA composites with HAp and Mg-HAp particles after 28 days in SBF was not detected.
PB  - Savez inženjera metalurgije Srbije, Beograd
T2  - Metallurgical & Materials Engineering
T1  - The effect of calcinated hydroxyapatite and magnesium doped hydroxyapatite as fillers on the mechanical properties of a model bisgma/tegdma dental composite initially and after aging
VL  - 24
IS  - 4
SP  - 271
EP  - 281
DO  - 10.30544/403
ER  - 
@article{
author = "Matić, Tamara and Ležaja-Zebić, Maja and Cvijović-Alagić, Ivana and Miletić, Vesna and Petrović, Rada and Janaćković, Đorđe and Veljović, Đorđe",
year = "2018",
abstract = "This study aimed to investigate the possibility of modifying model BisGMA/TEGDMA dental composite by substituting 10 wt. % of conventional glass fillers with bioactive fillers based on calcinated nanosized hydroxyapatite (HAp) and Mg-doped hydroxyapatite (Mg-HAp). HAp and Mg-HAp powders were synthesized hydrothermally. Mechanical properties: hardness by Vickers (HV) and flexural strength (Fs) were tested initially and after being stored for 28 days in simulated body fluid (SBF). The experimental composites with HAp and Mg-HAp particles showed no statistically significant difference in HV compared to the control (p>0.05) either initially or after storage. Although mean Fs values of modified composites tested initially were lower (62 MPa) than those of the control (72 MPa), after 28 days of storage in SBF Fs values were greater for modified composites (42 MPa control sample, 48 MPa HAp, and Mg-HAp samples). In vitro bioactivity of BisGMA/TEGDMA composites with HAp and Mg-HAp particles after 28 days in SBF was not detected.",
publisher = "Savez inženjera metalurgije Srbije, Beograd",
journal = "Metallurgical & Materials Engineering",
title = "The effect of calcinated hydroxyapatite and magnesium doped hydroxyapatite as fillers on the mechanical properties of a model bisgma/tegdma dental composite initially and after aging",
volume = "24",
number = "4",
pages = "271-281",
doi = "10.30544/403"
}
Matić, T., Ležaja-Zebić, M., Cvijović-Alagić, I., Miletić, V., Petrović, R., Janaćković, Đ.,& Veljović, Đ.. (2018). The effect of calcinated hydroxyapatite and magnesium doped hydroxyapatite as fillers on the mechanical properties of a model bisgma/tegdma dental composite initially and after aging. in Metallurgical & Materials Engineering
Savez inženjera metalurgije Srbije, Beograd., 24(4), 271-281.
https://doi.org/10.30544/403
Matić T, Ležaja-Zebić M, Cvijović-Alagić I, Miletić V, Petrović R, Janaćković Đ, Veljović Đ. The effect of calcinated hydroxyapatite and magnesium doped hydroxyapatite as fillers on the mechanical properties of a model bisgma/tegdma dental composite initially and after aging. in Metallurgical & Materials Engineering. 2018;24(4):271-281.
doi:10.30544/403 .
Matić, Tamara, Ležaja-Zebić, Maja, Cvijović-Alagić, Ivana, Miletić, Vesna, Petrović, Rada, Janaćković, Đorđe, Veljović, Đorđe, "The effect of calcinated hydroxyapatite and magnesium doped hydroxyapatite as fillers on the mechanical properties of a model bisgma/tegdma dental composite initially and after aging" in Metallurgical & Materials Engineering, 24, no. 4 (2018):271-281,
https://doi.org/10.30544/403 . .
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