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Microstructure and wettability of root canal dentine and root canal filling materials after different chemical irrigation

Authorized Users Only
2015
Authors
Antonijević, Đorđe
Milovanović, Petar
Brajković, Denis
Ilić, Dragan
Hahn, Michael
Amling, Michael
Rakocević, Zlatko
Đurić, Marija
Busse, Bjoern
Article (Published version)
Metadata
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Abstract
The objective of this study was to determine the effects of various irrigation solutions on root canal dentine and gutta-percha surface properties. In addition, the effects of disinfectant chemicals on the wettability and surface morphological properties of the filling materials were evaluated. Ethylenediaminetetraacetic acid (EDTA), citric acid, and ozone were employed as irrigation solutions for dentine and gutta-percha treatment. Thereafter, the samples' microstructure, degree of mineralization, and mechanical properties were assessed by means of quantitative backscattered electron imaging (qBEI) and reference point indentation (RN). A contact angle analyzer was used to measure adhesion on the tested materials. Here, EDTA had the most significant affect on both the mechanical properties and the adhesive behavior of dentine. Citric acid did not affect dentine wettability, whereas the indentation properties and the mineralization were reduced. Similar effects were observed when ozone ...was used. The dentinal tubules were significantly widened in citric acid compared to the ozone group. EDTA causes considerable micromechanical surface alteration of dentine and gutta-percha, but represents the best option in clinical cases where a high adhesiveness of the filling materials is desired.

Keywords:
EDTA / Citric acid / Ozone / Surface free energy / Reference point indentation / Quantitative backscattered electron microscopy
Source:
Applied Surface Science, 2015, 355, 369-378
Publisher:
  • Elsevier Science Bv, Amsterdam
Funding / projects:
  • German Academic Exchange Service, (DAAD)Deutscher Akademischer Austausch Dienst (DAAD)
  • Ministry of Education and Science of the Republic of Serbia
  • South-East-Europe Cooperation of University Medical Center Hamburg-Eppendorf
  • Functional, Functionalized and Advanced Nanomaterials (RS-45005)

DOI: 10.1016/j.apsusc.2015.07.023

ISSN: 0169-4332

WoS: 000363815700053

Scopus: 2-s2.0-84944321457
[ Google Scholar ]
5
5
URI
https://smile.stomf.bg.ac.rs/handle/123456789/1994
Collections
  • Radovi istraživača
Institution/Community
Stomatološki fakultet
TY  - JOUR
AU  - Antonijević, Đorđe
AU  - Milovanović, Petar
AU  - Brajković, Denis
AU  - Ilić, Dragan
AU  - Hahn, Michael
AU  - Amling, Michael
AU  - Rakocević, Zlatko
AU  - Đurić, Marija
AU  - Busse, Bjoern
PY  - 2015
UR  - https://smile.stomf.bg.ac.rs/handle/123456789/1994
AB  - The objective of this study was to determine the effects of various irrigation solutions on root canal dentine and gutta-percha surface properties. In addition, the effects of disinfectant chemicals on the wettability and surface morphological properties of the filling materials were evaluated. Ethylenediaminetetraacetic acid (EDTA), citric acid, and ozone were employed as irrigation solutions for dentine and gutta-percha treatment. Thereafter, the samples' microstructure, degree of mineralization, and mechanical properties were assessed by means of quantitative backscattered electron imaging (qBEI) and reference point indentation (RN). A contact angle analyzer was used to measure adhesion on the tested materials. Here, EDTA had the most significant affect on both the mechanical properties and the adhesive behavior of dentine. Citric acid did not affect dentine wettability, whereas the indentation properties and the mineralization were reduced. Similar effects were observed when ozone was used. The dentinal tubules were significantly widened in citric acid compared to the ozone group. EDTA causes considerable micromechanical surface alteration of dentine and gutta-percha, but represents the best option in clinical cases where a high adhesiveness of the filling materials is desired.
PB  - Elsevier Science Bv, Amsterdam
T2  - Applied Surface Science
T1  - Microstructure and wettability of root canal dentine and root canal filling materials after different chemical irrigation
VL  - 355
SP  - 369
EP  - 378
DO  - 10.1016/j.apsusc.2015.07.023
ER  - 
@article{
author = "Antonijević, Đorđe and Milovanović, Petar and Brajković, Denis and Ilić, Dragan and Hahn, Michael and Amling, Michael and Rakocević, Zlatko and Đurić, Marija and Busse, Bjoern",
year = "2015",
abstract = "The objective of this study was to determine the effects of various irrigation solutions on root canal dentine and gutta-percha surface properties. In addition, the effects of disinfectant chemicals on the wettability and surface morphological properties of the filling materials were evaluated. Ethylenediaminetetraacetic acid (EDTA), citric acid, and ozone were employed as irrigation solutions for dentine and gutta-percha treatment. Thereafter, the samples' microstructure, degree of mineralization, and mechanical properties were assessed by means of quantitative backscattered electron imaging (qBEI) and reference point indentation (RN). A contact angle analyzer was used to measure adhesion on the tested materials. Here, EDTA had the most significant affect on both the mechanical properties and the adhesive behavior of dentine. Citric acid did not affect dentine wettability, whereas the indentation properties and the mineralization were reduced. Similar effects were observed when ozone was used. The dentinal tubules were significantly widened in citric acid compared to the ozone group. EDTA causes considerable micromechanical surface alteration of dentine and gutta-percha, but represents the best option in clinical cases where a high adhesiveness of the filling materials is desired.",
publisher = "Elsevier Science Bv, Amsterdam",
journal = "Applied Surface Science",
title = "Microstructure and wettability of root canal dentine and root canal filling materials after different chemical irrigation",
volume = "355",
pages = "369-378",
doi = "10.1016/j.apsusc.2015.07.023"
}
Antonijević, Đ., Milovanović, P., Brajković, D., Ilić, D., Hahn, M., Amling, M., Rakocević, Z., Đurić, M.,& Busse, B.. (2015). Microstructure and wettability of root canal dentine and root canal filling materials after different chemical irrigation. in Applied Surface Science
Elsevier Science Bv, Amsterdam., 355, 369-378.
https://doi.org/10.1016/j.apsusc.2015.07.023
Antonijević Đ, Milovanović P, Brajković D, Ilić D, Hahn M, Amling M, Rakocević Z, Đurić M, Busse B. Microstructure and wettability of root canal dentine and root canal filling materials after different chemical irrigation. in Applied Surface Science. 2015;355:369-378.
doi:10.1016/j.apsusc.2015.07.023 .
Antonijević, Đorđe, Milovanović, Petar, Brajković, Denis, Ilić, Dragan, Hahn, Michael, Amling, Michael, Rakocević, Zlatko, Đurić, Marija, Busse, Bjoern, "Microstructure and wettability of root canal dentine and root canal filling materials after different chemical irrigation" in Applied Surface Science, 355 (2015):369-378,
https://doi.org/10.1016/j.apsusc.2015.07.023 . .

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